17.18 Methyl acetylene-propadiene mixtures
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17.18 Methyl acetylene-propadiene mixtures

  17.18.1 Methyl acetylene-propadiene mixtures should be suitably stabilized for transport. Additionally, upper limits of temperature and pressure during the refrigeration should be specified for the mixtures.

  17.18.2 Examples of acceptable, stabilized compositions are:

  • .1 Composition 1

    • .1.1 maximum methyl acetylene to propadiene molar ratio of 3 to 1;

    • .1.2 maximum combined concentration of methyl acetylene and propadiene of 65 mol per cent;

    • .1.3 minimum combined concentration of propane, butane, and isobutane of 24 mol per cent, of which at least one third (on a molar basis) must be butanes and one third propane; and

    • .1.4 maximum combined concentration of propylene and butadiene of 10 mol per cent.

  • .2 Composition 2

    • .2.1 maximum methyl acetylene and propadiene combined concentration of 30 mol per cent;

    • .2.2 maximum methyl acetylene concentration of 20 mol per cent;

    • .2.3 maximum propadiene concentration of 20 mol per cent;

    • .2.4 maximum propylene concentration of 45 mol per cent;

    • .2.5 maximum butadiene and butylenes combined concentration of 2 mol per cent;

    • .2.6 minimum saturated C4 hydrocarbon concentration of 4 mol per cent; and

    • .2.7 minimum propane concentration of 25 mol per cent.

  17.18.3 Other compositions may be accepted provided the stability of the mixture is demonstrated to the satisfaction of the Administration.

  17.18.4 A ship carrying methyl acetylene-propadiene mixtures should preferably have an indirect refrigeration system as specified in 7.2.4.2. Alternatively, a ship not provided with indirect refrigeration may utilize direct vapour compression refrigeration subject to pressure and temperature limitations depending on the composition. For the example compositions given in 17.18.2, the following features should be provided:

  • .1 A vapour compressor that does not raise the temperature and pressure of the vapour above 60°C and 17.5 bar gauge during its operation, and that does not allow vapour to stagnate in the compressor while it continues to run.

  • .2 Discharge piping from each compressor stage or each cylinder in the same stage of a reciprocating compressor should have:

    • .2.1 two temperature-actuated shutdown switches set to operate at 60°C or less;

    • .2.2 a pressure-actuated shutdown switch set to operate at 17.5 bar gauge or less; and

    • .2.3 a safety relief valve set to relieve at 18.0 bar gauge or less.

  • .3 The relief valve required by 17.18.4.2.3 should vent to a mast meeting the requirements of 8.2.9, 8.2.10, 8.2.13 and 8.2.14 and should not relieve into the compressor suction line.

  • .4 An alarm that sounds in the cargo control position and in the navigating bridge when a high-pressure switch, or a high-temperature switch operates.

  17.18.5 The piping system, including the cargo refrigeration system, for tanks to be loaded with methyl acetylene-propadiene mixtures should be either independent (as defined in 1.3.20) or separate (as defined in 1.3.32) from piping and refrigeration systems for other tanks. This segregation applies to all liquid and vapour vent lines and any other possible connections, such as common inert gas supply lines.


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